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Beilstein J. Org. Chem. 2008, 4, No. 6, doi:10.1186/1860-5397-4-6
Graphical Abstract
Figure 1: Subclasses of diastereoisomeric 5,8-disubstituted alkaloids. The absolute stereochemistry of 5,9Z-2...
Scheme 1: Reagents: (i) MeMgI. 96% (ii) PTSA 71%. (iii) TiCl4 CH2Cl2 25 oC 3d 68%. (iv) MsCl, Et3N, THF -40 o...
Figure 2: EIMS spectra of a) natural 5,9E-259B, b) synthetic 7, and c) synthetic minor diastereomer of 7. Str...
Figure 3: Vapor-phase FTIR spectra of a) natural 5,9E-259B, and b) synthetic 7. Structure shown with relative...